Details
Quality Manufacturer Supply High Purity 99% 10-Bromodecanol 53463-68-6 with Reasonable Price
- Molecular Formula: C10H21BrO
- Molecular Weight: 237.18
- Appearance/Colour: Clear yellow liquid
- Vapor Pressure: 0.000257mmHg at 25°C
- Refractive Index: n20/D 1.476(lit.)
- Boiling Point: 288.588 °C at 760 mmHg
- PKA: 15.20±0.10(Predicted)
- Flash Point: 118.313 °C
- PSA： 20.23000
- Density: 1.161 g/cm3
- LogP: 3.49440
10-Bromodecanol(Cas 53463-68-6) Usage
InChI:InChI=1/C10H21BrO/c11-9-7-5-3-1-2-4-6-8-10-12/h12H,1-10H2
53463-68-6 Relevant articles
Hydroxyl-Assisted trans-Reduction of 1,3-Enynes: Application to the Formal Synthesis of (+)-Aspicilin
Schaubach, Sebastian,Michigami, Kenichi,Fürstner, Alois
, p. 202 - 208 (2017)
1,3-Enynes are hardly amenable to trans-...
Synthesis of ent-BE-43547A 1 reveals a potent hypoxia-selective anticancer agent and uncovers the biosynthetic origin of the APD-CLD natural products
Villadsen, Nikolaj L.,Jacobsen, Kristian M.,Keiding, Ulrik B.,Weibel, Esben T.,Christiansen, Bj?rn,Vosegaard, Thomas,Bjerring, Morten,Jensen, Frank,Johannsen, Mogens,T?rring, Thomas,Poulsen, Thomas B.
, p. 264 - 272 (2017)
Tumour hypoxia is speculated to be a key...
Improvement of antimalarial activity of a 3-alkylpiridine alkaloid analog by replacing the pyridine ring to a thiazole-containing heterocycle: Mode of action, mutagenicity profile, and Caco-2 cell-based permeability
Guimar?es, Daniel Silqueira Martins,de Sousa Luz, Letícia Silveira,do Nascimento, Sara Batista,Silva, Lorena Rabelo,de Miranda Martins, Natália Rezende,de Almeida, Heloísa Gon?alves,de Souza Reis, Vitória,Maluf, Sarah El Chamy,Budu, Alexandre,Marinho, Juliane Aparecida,Abramo, Clarice,Carmona, Adriana Karaoglanovic,da Silva, Marina Goulart,da Silva, Gisele Rodrigues,Kemmer, Victor Matheus,Butera, Anna Paola,Ribeiro-Viana, Renato Márcio,Gazarini, Marcos Leoni,Júnior, Clébio Soares Nascimento,Guimar?es, Luciana,dos Santos, Fabio Vieira,de Castro, Whocely Victor,Viana, Gustavo Henrique Ribeiro,de Brito, Cristiana Ferreira Alves,de Pilla Varotti, Fernando
, (2019)
The development of new antimalarial drug...
Toward the synthesis of the hypoxia selective anticancer agent BE-43547 A2
Kranthikumar, Ramagonolla
supporting information, p. 9833 - 9839 (2021/12/07)
A short and enantioselective synthesis o...
A New Asymmetric Synthesis of (S)-14-Methyloctadec-1-ene, the Sex Pheromone of the Peach Leafminer Moth
Bai, Hongjin,Du, Zhen-Ting,He, Guo-Guo,Liu, Lu,Tang, Meng,Wei, Liang,Zhang, Tao
, p. 1089 - 1095 (2020/07/25)
Abstract: An asymmetric synthesis of 14-...
Synthesis method of sex pheromone (S)-14-methyl-1-octadecene of lepidoptera pest peach leaf miners
-
Paragraph 0047; 0065-0066, (2020/08/02)
The invention discloses a synthesis meth...
Industrial synthesis method of dichocrocis punctiferalis sex pheromone
-
Paragraph 0023-0025, (2020/06/30)
The invention belongs to the field of ch...
53463-68-6 Process route
-
-
112-47-0
1,10-Decanediol
-
-
53463-68-6
1-bromo-10-decanol
-
-
4101-68-2
1,10-dibromodecane
| Conditions | Yield |
|---|---|
|
With
hydrogen bromide;
In
cyclohexane;
for 6h;
Heating;
|
9%
88% |
|
With
hydrogen bromide;
In
toluene;
for 48h;
Heating;
|
87%
|
|
With
hydrogen bromide;
In
water; toluene;
Reflux;
|
87%
|
|
With
hydrogen bromide;
|
73%
|
|
With
tetrabutylammomium bromide; hydrogen bromide;
In
water;
at 105 ℃;
for 2h;
chemoselective reaction;
|
64%
10% |
|
With
tetrabutylammomium bromide; hydrogen bromide;
In
water;
at 100 ℃;
for 0.0833333h;
Microwave irradiation;
|
45%
|
|
With
hydrogen bromide;
at 130 ℃;
|
|
|
With
hydrogen bromide;
In
para-xylene; water;
at 130 - 135 ℃;
for 6.5h;
Dean-Stark;
|
-
-
112-47-0
1,10-Decanediol
-
-
53463-68-6
1-bromo-10-decanol
| Conditions | Yield |
|---|---|
|
With
hydrogen bromide;
In
water; toluene;
for 16h;
Inert atmosphere;
Reflux;
Dean-Stark;
|
93%
|
|
With
hydrogen bromide;
In
water; toluene;
Reflux;
Inert atmosphere;
|
92%
|
|
With
hydrogen bromide;
In
water; toluene;
Reflux;
|
92%
|
|
With
hydrogen bromide;
In
toluene;
at 180 ℃;
for 24h;
|
92%
|
|
With
hydrogen bromide;
In
water; toluene;
for 72h;
Heating / reflux;
|
90%
|
|
With
hydrogen bromide;
In
water; toluene;
for 72h;
Heating / reflux;
|
90%
|
|
With
hydrogen bromide;
In
toluene;
for 16h;
Heating;
|
89%
|
|
With
hydrogen bromide;
In
cyclohexane; water;
for 6h;
Heating / reflux;
|
89%
|
|
With
hydrogen bromide;
In
toluene;
for 24h;
Reflux;
|
88.93%
|
|
With
hydrogen bromide;
In
toluene;
Reflux;
|
88.18%
|
|
With
hydrogen bromide;
In
water; Petroleum ether;
for 4h;
Heating / reflux;
|
87%
|
|
With
hydrogen bromide;
In
benzene;
for 28h;
Heating;
|
85%
|
|
With
hydrogen bromide;
In
toluene;
|
85%
|
|
With
hydrogen bromide;
In
toluene;
for 72h;
Reflux;
Inert atmosphere;
|
84%
|
|
With
hydrogen bromide;
In
toluene;
at 110 ℃;
for 24h;
|
84%
|
|
With
hydrogen bromide;
In
water; toluene;
at 95 - 97 ℃;
for 72h;
|
82%
|
|
With
hydrogen bromide;
In
water; toluene;
for 48h;
Reflux;
Inert atmosphere;
|
82%
|
|
With
hydrogen bromide;
|
81%
|
|
With
hydrogen bromide;
In
benzene;
for 30h;
Heating;
|
80%
|
|
With
hydrogen bromide;
In
benzene;
for 28h;
Heating;
|
80%
|
|
With
hydrogen bromide;
In
benzene;
Heating;
|
80%
|
|
With
tetrabutylammomium bromide; hydrogen bromide;
In
water;
for 0.0833333h;
Microwave irradiation;
|
80%
|
|
With
hydrogen bromide; tetra-(n-butyl)ammonium iodide;
In
water;
for 0.0833333h;
Microwave irradiation;
|
80%
|
|
With
hydrogen bromide;
In
water; toluene;
for 43h;
Inert atmosphere;
Reflux;
|
79%
|
|
With
hydrogen bromide;
at 85 ℃;
for 3h;
|
78%
|
|
With
hydrogen bromide;
|
78%
|
|
With
hydrogen bromide;
In
cyclohexane; water;
at 80 ℃;
for 5h;
Inert atmosphere;
|
78.5%
|
|
With
hydrogen bromide;
In
water; toluene;
for 6h;
Reflux;
|
77%
|
|
With
hydrogen bromide;
at 70 ℃;
for 40h;
|
74%
|
|
With
hydrogen bromide;
In
water; toluene;
for 36h;
Reflux;
|
74.5%
|
|
With
hydrogen bromide;
In
water; toluene;
for 48h;
Reflux;
|
74%
|
|
With
hydrogen bromide;
In
water; toluene;
for 16h;
Dean-Stark;
Reflux;
|
74%
|
|
With
hydrogen bromide;
In
water; toluene;
for 16h;
Reflux;
|
73%
|
|
With
hydrogen bromide;
In
n-heptane;
|
70%
|
|
With
hydrogen bromide;
In
n-heptane;
for 25h;
Heating;
|
70%
|
|
With
hydrogen bromide;
|
69%
|
|
In
hydrogen bromide;
|
69%
|
|
With
hydrogen bromide;
In
toluene;
Heating;
|
68%
|
|
With
hydrogen bromide;
In
ligroin;
for 72h;
|
67.1%
|
|
With
hydrogen bromide;
In
Petroleum ether;
at 90 - 95 ℃;
for 65h;
|
65%
|
|
With
hydrogen bromide;
In
benzene;
for 24h;
Heating;
|
63%
|
|
With
hydrogen bromide;
In
toluene;
at 20 ℃;
for 18h;
|
59%
|
|
With
hydrogen bromide;
In
water; toluene;
for 48h;
Reflux;
Inert atmosphere;
|
57%
|
|
With
hydrogen bromide;
In
water; toluene;
Reflux;
Dean-Stark;
|
57%
|
|
With
hydrogen bromide;
In
water; toluene;
at 90 - 95 ℃;
for 48h;
|
56%
|
|
With
hydrogen bromide;
|
48%
|
|
With
water; hydrogen bromide;
|
|
|
With
hydrogen bromide;
In
n-heptane;
Heating;
|
|
|
With
hydrogen bromide;
In
Petroleum ether;
|
|
|
With
hydrogen bromide;
In
toluene;
|
|
|
With
hydrogen bromide;
In
water;
for 60h;
Heating;
|
|
|
With
sulfuric acid; hydrogen bromide;
for 2h;
Heating;
|
|
|
With
hydrogen bromide;
In
n-heptane;
Heating;
|
|
|
With
hydrogen bromide;
In
cyclohexane;
for 6h;
Heating;
|
|
|
With
hydrogen bromide;
In
toluene;
for 72h;
Heating;
|
|
|
With
hydrogen bromide;
In
cyclohexane;
for 6h;
Heating;
|
|
|
In
hexane; hydrogen bromide;
|
|
|
In
hexane; hydrogen bromide;
|
|
|
With
hydrogen bromide;
In
toluene;
for 16h;
Reflux;
|
|
|
With
hydrogen bromide;
In
benzene;
for 2.5h;
Reflux;
|
73.47 mg
|
|
With
hydrogen bromide;
In
toluene;
for 75h;
Reflux;
|
|
|
With
hydrogen bromide;
In
toluene;
at 120 ℃;
for 16h;
|
|
|
With
hydrogen bromide;
In
water; toluene;
for 48h;
Reflux;
|
53463-68-6 Upstream products
-
112-47-0
1,10-Decanediol
-
50530-12-6
10-bromodecanoic acid
-
51309-10-5
10-chlorodecanol
-
1124-78-3
1Z,5E-cyclodecadiene
53463-68-6 Downstream products
-
70869-30-6
10-Hydroxydecyl-dithio-p-toluat
-
51795-88-1
1-bromo-10-(tetrahydropyranyloxy)decane
-
84999-79-1
1-hydroxy octadec 11-yne
-
132841-87-3
10-(phenylselanyl)decan-1-ol
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