Details
Manufacturer supply 3-Bromomethylthiophene 34846-44-1 with sufficient stock and high standard
- Molecular Formula: C5H5BrS
- Molecular Weight: 177.065
- Vapor Pressure: 0.527mmHg at 25°C
- Melting Point: -9 °C
- Refractive Index: 1.603
- Boiling Point: 197.6 °C at 760 mmHg
- Flash Point: 73.3 °C
- PSA： 28.24000
- Density: 1.633 g/cm3
- LogP: 2.64300
3-Bromomethylthiophene(Cas 34846-44-1) Usage
InChI:InChI=1/C5H5BrS/c6-3-5-1-2-7-4-5/h1-2,4H,3H2
34846-44-1 Relevant articles
Synthesis and characterization of block copolythiophene with hexyl and triethylene glycol side chains
Higashihara, Tomoya,Ohshimizu, Kaoru,Ryo, Yecheol,Sakurai, Takuya,Takahashi, Ayumi,Nojima, Shuichi,Ree, Moonhor,Ueda, Mitsuru
, p. 3687 - 3695 (2011)
A well-defined diblock copolythiophene, ...
Transient Photoconductivity of Acceptor-Substituted Poly(3-butylthiophene)
Greenwald, Y.,Cohen, G.,Poplawski, J.,Ehrenfreund, E.,Speiser, S.,Davidov, D.
, p. 2980 - 2984 (1996)
We have studied acceptor-substituted pol...
Synthesis and pharmacological characterisation of arctigenin analogues as antagonists of AMPA and kainate receptors
Butts, Craig P.,Collingridge, Graham L.,Jane, David E.,Mallah, Shahida,Molnár, Elek,Re?nik, Lisa-Maria,Thatcher, Robert J.,Willis, Christine L.
supporting information, p. 9154 - 9162 (2021/11/16)
(-)-Arctigenin and a series of new analo...
Preparation method 3- thiophene formaldehyde
-
Paragraph 0044-0045; 0047-0048; 0050-0051; 0053-0054, (2020/03/23)
The preparation method disclosed by the ...
Opioid receptor agonists and application thereof
-
Paragraph 1968; 1971-1975; 2008; 2012-2017, (2019/01/24)
The invention discloses compounds and sa...
Silver-Assisted Oxidative Isocyanide Insertion of Ethers: A Direct Approach to β-Carbonyl α-Iminonitriles
Zhao, Leiyang,Liu, Bingxin,Tan, Qitao,Ding, Chang-Hua,Xu, Bin
supporting information, p. 9223 - 9227 (2019/11/14)
An efficient silver-assisted oxidative c...
34846-44-1 Process route
-
-
71637-34-8
3-hydroxymethyl-thiophene
-
-
34846-44-1
3-Bromomethylthiophene
| Conditions | Yield |
|---|---|
|
With
phosphorus tribromide;
In
dichloromethane;
at 20 ℃;
for 16h;
Inert atmosphere;
|
100%
|
|
With
phosphorus tribromide;
In
benzene;
for 3h;
Ambient temperature;
|
89%
|
|
With
1H-imidazole; bromine; triphenylphosphine;
In
dichloromethane;
at 0 - 20 ℃;
Inert atmosphere;
|
89%
|
|
With
pyridine; bromine; triphenylphosphine;
In
dichloromethane;
at 0 ℃;
|
73%
|
|
With
phosphorus tribromide;
In
dichloromethane;
at 20 ℃;
for 16h;
|
70%
|
|
With
hydrogen bromide;
for 3h;
|
70%
|
|
With
phosphorus tribromide;
In
dichloromethane;
at 20 ℃;
|
23%
|
|
With
phosphorus tribromide;
In
dichloromethane;
at 0 - 20 ℃;
for 3h;
|
|
|
With
dibromotriphenylphosphorane;
Inert atmosphere;
|
|
|
With
hydrogen bromide;
Cooling with ice;
|
|
|
With
phosphorus tribromide;
In
diethyl ether;
at 0 ℃;
for 0.5h;
|
|
|
With
carbon tetrabromide; triphenylphosphine;
In
dichloromethane;
at 20 ℃;
for 3h;
|
|
|
With
phosphorus tribromide;
In
dichloromethane;
at 20 ℃;
for 24h;
|
|
|
With
phosphorus tribromide;
In
diethyl ether;
at 25 ℃;
for 12h;
|
-
-
616-44-4,84928-92-7
3-Methylthiophene
-
-
34846-44-1
3-Bromomethylthiophene
| Conditions | Yield |
|---|---|
|
With
N-Bromosuccinimide; dihydrogen peroxide;
In
tetrachloromethane;
|
90%
|
|
With
N-Bromosuccinimide; dibenzoyl peroxide;
In
benzene;
for 0.5h;
Heating;
|
88%
|
|
With
N-Bromosuccinimide; dibenzoyl peroxide;
In
tetrachloromethane;
for 2h;
Reflux;
|
87%
|
|
With
N-Bromosuccinimide;
In
tetrachloromethane;
for 0.666667h;
Heating;
Irradiation;
|
78%
|
|
With
N-Bromosuccinimide;
|
75%
|
|
With
N-Bromosuccinimide; dibenzoyl peroxide;
In
tetrachloromethane;
at 70 ℃;
for 2h;
|
75%
|
|
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile);
In
tetrachloromethane;
for 5h;
Heating;
Irradiation;
|
74%
|
|
With
N-Bromosuccinimide; dibenzoyl peroxide;
In
tetrachloromethane;
for 3h;
Heating / reflux;
|
71%
|
|
With
N-Bromosuccinimide; dibenzoyl peroxide;
In
benzene;
Heating;
|
64%
|
|
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile);
In
tetrachloromethane;
for 2h;
Reflux;
|
57%
|
|
|
56%
|
|
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile);
In
tetrachloromethane;
for 5h;
Reflux;
|
53%
|
|
With
N-Bromosuccinimide; dibenzoyl peroxide;
|
9%
|
|
With
N-Bromosuccinimide; benzene; dibenzoyl peroxide;
|
|
|
With
tetrachloromethane; N-Bromosuccinimide; dibenzoyl peroxide;
|
|
|
With
N-Bromosuccinimide;
Irradiation;
|
|
|
With
N-Bromosuccinimide; Perbenzoic acid;
In
tetrachloromethane;
|
|
|
With
N-Bromosuccinimide;
In
tetrachloromethane;
initiator: benzoyl peroxide;
|
|
|
With
N-Bromosuccinimide;
In
tetrachloromethane;
for 2h;
Heating;
Irradiation;
|
|
|
With
N-Bromosuccinimide; dibenzoyl peroxide;
In
tetrachloromethane;
for 0.433333h;
Heating;
|
81.6 g
|
|
With
N-Bromosuccinimide; dibenzoyl peroxide;
In
benzene;
at 90 ℃;
for 1.5h;
|
|
|
With
N-Bromosuccinimide; dibenzoyl peroxide;
In
tetrachloromethane;
for 2h;
Heating / reflux;
|
|
|
With
N-Bromosuccinimide; dibenzoyl peroxide;
at 100 ℃;
for 1h;
|
|
|
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile);
In
tetrachloromethane;
for 1h;
Reflux;
|
|
|
With
N-Bromosuccinimide;
In
tetrachloromethane;
|
|
|
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile);
In
ethyl acetate;
at 70 ℃;
for 2h;
Solvent;
|
34846-44-1 Upstream products
-
56-23-5
tetrachloromethane
-
128-08-5
N-Bromosuccinimide
-
616-44-4
3-Methylthiophene
-
94-36-0
dibenzoyl peroxide
34846-44-1 Downstream products
-
91-79-2
N ,N -dimethyl-N '-[2]pyridyl-N '-[3]thienylmethyl-ethylenediamine
-
13781-53-8
(thiophen-3-yl)acetonitrile
-
6964-21-2
thiophen-3-yl-acetic acid
-
109106-67-4
2-(thiophen-3-ylmethyl)phenol
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